Powder amino heat treatment

We investigated the use of the molding resin powder (<150 m) as a filler for construction materials composed of bisphenol A type epoxy resin and amine type hardener, and compared the material properties with those produced with a silica powder filler (<150 fi m). Furthermore, the effect of surface treatment of the molding resin powder on these properties was examined by using epoxy or amino silane coupling agents, which were added at lwt% to the molding resin powder and heated at 100°C for 1 hr. 

The worst substrate tested was milk powder. This probably occurred due to its thin granularity, which ends up allowing a gathering of the particles when moist, causing stickiness. Moreover, the heat treatment during sterilization may have promoted Maillard reactions, which maybe affected the availability of amino acids in the medium, and also caramelization reactions, both leading to a darkening and modification of the medium s texture. 

Simultaneously with Hansa Yellow G, compound 84 was first described as early as 1909 by Farbenfabriken Bayer. Its preparation starts from l-amino-4-bro-moanthraquinone-2-sulfonic acid (bromamine acid) 85. Dimerization is achieved through the Ullmann reaction, i.e., treatment with fine-grain copper powder in dilute sulfuric acid at 75°C. The separated intermediate, the disodium salt of 4,4 -diamino-l,l -dianthraquinonyl-3,3 -disulfonic acid 86, is heated to 135 to 140°C in the presence of 80% sulfuric acid in order to cleave the sulfonic acid groups [7] ... 

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