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PHOSPHORUS THIOCHLORIDE

Preparation of Phosphorus Thiochloride. Put 33 ml of phosphorus trichloride and 12 g of finely triturated sulphur into flask 1 (Fig. 103). Place 3 g of anhydrous aluminium chloride into test tube 3. [Pg.162]

Pour the reaction mixture into the flask of an apparatus for fractional distillation under atmospheric pressure (see Fig. 20). Collect the fraction boiling at 125 °C. Pour the phosphorus thiochloride into a weighed drawn out test tube. Seal the ampoule wear eye protection ). Weigh the ampoule and the remaining parts of the test tube. Write the equation of the reaction. Calculate the yield in per cent. Test the reaction of phosphorus thiochloride with water. Write the equation of the reaction. What is the oxidation state of sulphur in this compound ... [Pg.162]

GaCI3 gallium trichloride 13450-90-3 3.479 3398 PSCI3 phosphorus thiochloride 3982-91-0 3.634... [Pg.670]

PSC13 phosphorus thiochloride 3982-91-0 gas 1.420 1 4275 Si2C6H19N disilazane, hexamethyl 999-97-3 in benzene 0.420 1... [Pg.685]

PSC13 PHOSPHORUS THIOCHLORIDE 27.454 3.3554E-01 -5.4132E-04 3.7986E-07 -9.6538E-11 100 1500 gas... [Pg.360]

A soln. of phosphorus thiochloride in ether added dropwise with water-cooling ... [Pg.206]

See other pages where PHOSPHORUS THIOCHLORIDE is mentioned: [Pg.206]    [Pg.218]    [Pg.224]    [Pg.290]    [Pg.628]    [Pg.161]    [Pg.411]    [Pg.411]    [Pg.1066]    [Pg.1068]    [Pg.355]    [Pg.361]    [Pg.102]    [Pg.204]    [Pg.406]    [Pg.550]    [Pg.647]    [Pg.787]    [Pg.307]    [Pg.628]    [Pg.355]    [Pg.361]    [Pg.451]    [Pg.481]    [Pg.223]    [Pg.354]    [Pg.223]    [Pg.354]    [Pg.161]    [Pg.598]    [Pg.598]    [Pg.223]   
See also in sourсe #XX -- [ Pg.223 ]

See also in sourсe #XX -- [ Pg.223 ]

See also in sourсe #XX -- [ Pg.13 , Pg.15 , Pg.490 , Pg.636 ]



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Thiochloride

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