Nuclear magnetic resonance spectroscopy sohd state

Tycko, R. Molecular dynamics, phase diagrams and electronic properties of fuller-enes and alkali fullerides Insights from sohd-state nuclear magnetic resonance spectroscopy.. Solid State Nud. Masn. Reson. 1994 3 303-314. 

Simpson, M. J., and Hatcher, P. G. (2004). Determination of black carbon in natural organic matter by chemical oxidation and sohd-state nC nuclear magnetic resonance spectroscopy. Org. Geochem. 35, 923-935. 

Cody, G. D., Alexander, C. M. O., and Tera, F. (2002). Sohd-state ( H and C) nuclear magnetic resonance spectroscopy of insoluble organic reside in the Muchison meterorite A self-consistent quantitative analysis. Geochim. Cosmochim. Acta 66(10), 1851—1865. 

Ulrich, A. S. (2005) Sohd state 19F-NMR methods for studying biomembranes. Progress in Nuclear Magnetic Resonance Spectroscopy, 46, 1-21. 

P. S. Belton, S. F. Tanner, N. Cartier, and H. Chanzy, High-resolution sohd-state C nuclear magnetic resonance spectroscopy of tunicin, an animal cellulose. Macromolecules, 22 (1989) 1615-1617. 

L. Vugmeyster, D. Ostrovsky,. . Ford, S.D. Burton, A.S. Lipton, G.L. Hoatson, R.L. Void, Probing the dynamics of a protein hydrophobic core by deuteron sohd-state nuclear magnetic resonance spectroscopy,. Am. Chem. Soc. 131 (2009) 13651-13658. 

R99 T. J. Bootten, P. J. Harris, L. D. Melton and R. H. Newman, Using Sohd-State C Nuclear Magnetic Resonance Spectroscopy to Study the Molecular Organisation of Primary Plant Cell Walls , in Methods in Molecular Biology (New York, NY, United States), ed. Z. A. Popper, Springer, 2011, Vol. 715, Plant Cell Wall - Methods and Protocols, p. 179. 

T.G. Oas, R.G. Griffin, M.H. Levitt, Rotary resonance recoupling of dipolar interactions in sohd-state nuclear magnetic resonance spectroscopy, J. Chem. Phys. 89 (1988) 692-695. 

Co-crystal patents usually contain experimental examples that describe the preparation of the co-crystal and the characterization of the co-crystal. Characterization of the co-crystal describes the co-crystal itself and its various properties which include its sohd state characteristics and stoichiometry. Typically, the sohd state characteristics of a crystalline solid are shown by one or more of the foUowing analytical techniques X-ray powder diffraction pCRPD), single crystal X-ray diffraction (SCXD), Raman spectroscopy, infrared (IR) spectroscopy, sohd state nuclear magnetic resonance spectroscopy (SSNMR), and differential scanning calorimetry (DSC). The stoichiometry of a co-crystal may be estabhshed through solution techniques such as comparison of peak integrations in a solution NMR spectrum, data... 

Two books entitled SoHd-State NMR Techniques and Nuclear Magnetic Resonance Spectroscopy of Cement-Based Materials , have been published. A number of reviews have appeared, entitled Solid-state nuclear magnetic resonance , Solid-state NMR spectroscopy of non-integer spin nuclei , A... 

B. Bureau, G. Silly, J.-Y. Buzare, J. Emery, C. Legein, C. Jacoboni, Investigation of fluorine octahedron connectivities in transition metal fluoride glasses by sohd-state magic-anglespinning nuclear magnetic resonance spectroscopy, J. Phys. Condens. Matter, 79,6719-6736 (1997). 

Hunger M, Wang W. Characterization of sohd catalysts in the functioning state by nuclear magnetic resonance spectroscopy. Adv Catal 2006 50 149-225. 

Ghassemzadeh, L., Marrony, M., Barrera, R., Kreuer, K. D., Maier, J., Muller, K., Chemical degradation of proton conducting perflurosulfonic acid ionomer membranes studied by sohd-state nuclear magnetic resonance spectroscopy. J. Power Sources 2009, 186 (2), 334-338. 

These ideas have been extended using new analytical techniques, in particular molecular modeling and soHd-state nuclear magnetic resonance (nmr) spectroscopy. 

The melting points, optical rotations, and uv spectral data for selected prostanoids are provided in Table 1. Additional physical properties for the primary PGs have been summarized in the Hterature and the physical methods have been reviewed (47). The molecular conformations of PGE2 and PGA have been determined in the soHd state by x-ray diffraction, and special H and nuclear magnetic resonance (nmr) spectral studies of several PGs have been reported (11,48—53). Mass spectral data have also been compiled (54) (see Mass spectrometry Spectroscopy). 

Ulrich, A. S., Wadhwani, P., Durr, U. H. N., el al. (2006) Sohd-state 19F-nuclear magnetic resonance analysis of membrane-active peptides, in NMR Spectroscopy of Biological Solids (ed. A. Ramamoorthy), CRC Press, Boca Raton, FL, pp. 215-236. 

Framework and Surfaces Since compositions and structures are very diverse, surface and framework properties are also extremely varied. In terms of compositions, coordination, and chemical environments, several methods are particularly informative for the characterization of nanoporous solids, such as nuclear magnetic resonance methods (NMR), UV-visible spectroscopy, Fourier-transform infrared spectroscopy (FTIR), Raman spectroscopy, x-ray absorption spectroscopies, x-ray photoelectron emission spectroscopy (XPS), and electron paramagnetic resonance (EPR) (4, 6). Among them, sohd state NMR techniques arc largely employed and will be briefly described in the following. 

Usami T, Itoh T, Ohtani H, Tsuge S, Structural study of polyacrylonitrile fibers during oxidative thermal degradation by Pyrolysis—Gas Chromatography, Sohd State C Nuclear Magnetic Resonance and Fourier Transform Infrared Spectroscopy, Macromolecules, 23, 2460 2465, 1990. 

Jager, W. R, Lungu, A., Chen, D. Y, and Neckers, D. C. 1997. Photopolymerization of polyfunctional acrylates and methacrylate mixtures Characterization of polymeric networks by a combination of fluorescence spectroscopy and sohd state nuclear magnetic resonance. Macromolecules 30 780-91. 

---