Multidimensional Solid-State NMR Spectra

Here coj, is the Larmor frequency, A describes the strength of the anisotropic coupling i.e. the anisotropic chemical shift or dipole-dipole coupling for 

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Progress in multidimensional solid-state NMR has been hampered by experimental and conceptual difficulties, but these are now overcome [11-14]. This chapter briefly outlines some of the main concepts and illustrates the information avaUable from multidimensional solid-state NMR spectra concerning polymer structure and dynamics through experimental examples selected from the author s laboratory. 

Figure 5 Multidimensional solid-state NMR spectra of uniformly labelled fd coat protein in oriented lipid bilayers. Panel (A) is the complete two-dimensional heteronuclear dipolar-...

Nadaud PS, Helmus JJ, Sengupta I, Jaroniec CP (2010) Rapid acquisition of multidimensional solid-state NMR spectra of proteins facilitated by covalently bound paramagnetic tags. J Am Chem Soc 132 9561-9563... 

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