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Methyl 3-trimethylsiloxy-2-butenoate

Methyl 3-trimethylsiloxy-2-butenoate. This reagent silylates primary, secondary, and tertiary alcohols at room temperature without added catalyst. [Pg.70]

Mol. wt. 260.48, b.p. 56-5872.0 mm. The diene can be obtained by reaction of the enolatc of methyl 3-trimethylsiloxy-2-butenoate (n-BuLi, TMEDA, THF) with chlorotrimelhylsilane (91-98% yield). An alternate preparation has been published.2... [Pg.257]

Methyl 3-trimethylsiloxy-2-butenoate, 257 Methyl trioctylammonium chloride, 305 Methyl vinyl ketone, 272 Michael reactions, 9, 12, 27, 42, 81-82, 113-114, 196-197, 219, 223, 235-236, 266... [Pg.264]


See also in sourсe #XX -- [ Pg.257 ]




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Butenoic 3-methyl

Trimethylsiloxy

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