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Long-range COSY

FIGURE 25. A partial structure of lagunamycin (76) as revealed by H- H COSY, NOESY and H- C long-range COSY experiments. Reproduced by permission of Japan Antibiotics Research Association from Reference 46... [Pg.121]

Check it in 2D WIN-NMR C/H-long range-COSY (HMBC, magnit. mode)... [Pg.144]

Repeat the same procedure to plot the other C/H-long-range COSY spectra ... [Pg.144]

Figure 5.55. The delayed (or long-range) COSY sequence. Additional fixed delays are inserted into the basic COSY sequence to enhance the appearance of correlations from small couplings (see text). Figure 5.55. The delayed (or long-range) COSY sequence. Additional fixed delays are inserted into the basic COSY sequence to enhance the appearance of correlations from small couplings (see text).
Long-range COSY experiment for detection of small coupling constants... [Pg.286]

SDA (4), C27H3406, mp 172-174°C, [oc]d-5.7° (MeOH), was obtained as colorless prisms. All spectral data including H- H COSY,, 3C- H COSY and, 3C- H long-range COSY spectra of SDA suggested the presence of a... [Pg.692]

Fig. (11). Correlation in long range COSY spectrum, and significant enhancement of... Fig. (11). Correlation in long range COSY spectrum, and significant enhancement of...
Furthermore, from the knots of Wistaria brachybotrys, several kinds of oleanane type saponins (101 - 108) were isolated together with isoflavonoids. Of these saponins, wistariasaponins A, Bl, B2, C, D and G were found to be novel saponins, and their structures of sapogenols were elucidated by the long-range COSY spectra and difference NOE... [Pg.247]

The basic skeleton of casearin A (12) was elucidated by H-iH and H-correlated spectroscopy (COSY) and 2D-incredible natural abundance double quantum transfer experiment (INADEQUATE). The positions of ester functions were determined by the long range COSY... [Pg.280]

The locations of the acyl groups on the two glucose residues were assigned by the long-range COSY spectra of camelliatannin D (67)... [Pg.441]

Delayed COSY Correlating coupled homonuclear spins through small couplings. Often used to identify proton correlations over many bonds (>3), hence also known as long-range COSY... [Pg.130]


See other pages where Long-range COSY is mentioned: [Pg.313]    [Pg.393]    [Pg.333]    [Pg.117]    [Pg.349]    [Pg.23]    [Pg.216]    [Pg.137]    [Pg.182]    [Pg.253]    [Pg.117]    [Pg.117]    [Pg.121]    [Pg.145]    [Pg.148]    [Pg.229]    [Pg.148]    [Pg.189]    [Pg.199]    [Pg.285]    [Pg.286]    [Pg.287]    [Pg.288]    [Pg.276]    [Pg.692]    [Pg.648]    [Pg.252]    [Pg.137]    [Pg.225]    [Pg.234]    [Pg.438]    [Pg.157]    [Pg.159]    [Pg.166]   
See also in sourсe #XX -- [ Pg.182 , Pg.207 , Pg.253 ]




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COSY

Long range

Long range heteronuclear COSY

Long range heteronuclear COSY spectrum

Long-range COSY coupling

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