L-Aminoadamantine-2-ethanol

Preparation of the p-chlorophenoxyacetate of l-aminoadamantine-2-ethanol, starting from a p-chlorophenoxyacetic acid halide ... 

In a 1 liter flask, provided with a Dean-Stark separator tube and reflux refrigerant, a mixture of 20.5 g (0.011 m) of p-chlorophenoxyacetic acid, 22 g (0.11 m) of l-aminoadamantine-2-ethanol, 98 g of cone, sulfuric acid and 700 ml of toluene is heated to boiling point over a period of 24 hours. At the end... 

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