Hydroxylamine/Tert-Butyl Alcohol

Aldehydes Determine as directed in the Hydroxylamine/ Tert-Butyl Alcohol Method under Aldehydes and Ketones, Appendix VI, using about 5 mL of sample, accurately weighed, and 76.12 as the equivalence factor (e) in the calculation. Allow the mixture to stand at room temperature for 1 h before titrating. 

M-2a Aldehydes—Hydroxylamine tert-Butyl Alcohol Method... 

Alcoholic Sulfuric Acid, 0.5 N, 859 Alcoholic Sulfuric Acid, 5 N, 859 Alcohols, Total, 815 ALDC Activity, (S3)110 Aldehyde C-6, 504 Aldehyde C-7, 502, (S3)76 Aldehyde C-8, 540 Aldehyde C-9, 538 Aldehyde C-10, 476 Aldehyde C-ll Undecyclic, 560 Aldehyde C-ll Undecylenic, 560 Aldehyde C-12,518 Aldehyde C-12 MNA, 534 Aldehyde C-14 Pure, So-Called, 560 Aldehyde C-16, 492 Aldehyde C-18, So-Called, 538 Aldehyde-Free Alcohol, 849 Aldehydes and Ketones, 816 Hydroxylamine Method, 816 Hydroxylamine/Tert-Butyl Alcohol Method, 816... 

Aldehydes—Hydroxylamine/Tert-Butyl Alcohol Method, 564 Ketones—Hydroxylamine Method, 565 Procedure Requiring the Use of Sealed Glass Vials or Ampules, 564... 

Hydroxylamine Solution Dissolve 45 g of reagent-grade hydroxylamine hydrochloride in 130 mL of water, add 850 mL of tert-butyl alcohol, mix, and using a pH meter, neutralize to a pH of 3.0 to 3.5 with sodium hydroxide. 

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