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Hydrochloric Acid HCI

If one is absolutely serious about ultra pure safrole then it can be separated from the eugenol-free sassafras oil by treatment with mercuric acetate [1,2,3,4] which likes that terminal double bond that only safrole has. The Hg(AcO)2 latches on to safrole at that double bond bringing it into solution as a solid sort of like the way that eugenol was. The safrole can then be separated from its still oily buddies by vacuum filtration. Safrole is then regenerated to its normal oily form by treatment with hydrochloric acid (HCI) which flicks the Hg(AcO)2 off the safrole and the safrole double bond reforms. As it so happens, the mercuric acetate also reforms intact so that it can be reused again such as in one of those... [Pg.34]

Spray solution Ilb Dissolve 1 g 7V-(l-naphthyl)ethylenediamine dihydrochloride in 50 ml dimethylformamide and 50 ml hydrochloric acid (< Hci = 4 mol/1) with warming. If the cooled solution is not clear it should be filtered. A pale violet coloration does not interfere with the reaction [4]. [Pg.223]

Please pass the sodium chloride It is amazing that food is seasoned with an ionic compound that is composed of two deadly elements— sodium and chlorine. The gain or loss of electrons can make a big difference in properties. Reacting sodium hydrogen carbonate, which is baking soda, with hydrochloric acid (HCI), the acid found in your stomach, produces salt, carbon dioxide, and water, according to the following equation ... [Pg.61]

M hydrochloric acid (HCI) test tubes (6) test-tube rack... [Pg.73]

An example of a chemical reaction with a measurable energy change is the reaction of an acid and a base. In this activity, you will determine whether the reaction of hydrochloric acid (HCI) with sodium hydroxide (NaOH) absorbs or liberates heat. [Pg.121]

A chemical equation shows that as a chemical reaction takes place, reactants are changed into products. The reaction rate of a chemical reaction is often expressed as the change in concentration of a reactant or a product in a unit amount of time. In this activity, the reaction rate will be calculated from the amount of time it takes for a given amount of magnesium (Mg) to react completely with hydrochloric acid (HCI). [Pg.129]

A. 4-[(Bromophenyl)azo]morpholine. In a 500-mL Erlenmeyer flask equipped with a magnetic stirring bar are placed 4-bromoaniline (15.0 g, 87 mmol, Note 1) and 6 N hydrochloric acid (HCI), 36.4 mL, 210 mmol) and the mixture is warmed on a water bath to make a clear solution. It is cooled to 0°C to produce a heavy precipitate. A solution of sodium nitrite (6.30 g, 91 mmol) in water (10 mL) is added dropwise over 10 min. Stirring is continued at 0°C for 20 min (Note 2), and morpholine (8.3 g, 9.0 mL, 96 mmol) is added dropwise to the above solution over 10 min. Water (100 mL) is added followed by the... [Pg.27]

The toluene solution is cooled to 10-15°C and hydrochloric acid (HCI) in 2-propanol (0.275 mol) (Note 7) is added slowly over 1 hr via a pressure-equalizing dropping funnel, keeping the internal temperature below 25°C (Note 8). During the acid addition the product precipitates as its hydrochloride salt. The mixture is stirred at room temperature under nitrogen for 2 hr, and is reduced in volume by distillation under reduced pressure (45-50°C, 25-30 mm) with mechanical stirring to produce a distillate of approximately 120 mL and a residual volume of about 100 mL. Toluene (50 mL) is added and the slurry is reconcentrated under reduced pressure (45-50°C, 25-30 mm) until a residual volume of 100 mL is obtained. This process is repeated once more (Note 9). Toluene is added to adjust the total volume to about 250 mL. The mixture is then cooled to 10-15°C and stirred under nitrogen at this temperature for 2 hr. The HCI salt is isolated by filtration and the wet cake is washed with toluene (2 x 50 mL). [Pg.13]


See other pages where Hydrochloric Acid HCI is mentioned: [Pg.134]    [Pg.620]    [Pg.55]    [Pg.61]    [Pg.28]    [Pg.163]    [Pg.77]    [Pg.77]    [Pg.93]    [Pg.121]    [Pg.129]    [Pg.129]    [Pg.137]    [Pg.137]    [Pg.141]    [Pg.153]    [Pg.43]    [Pg.43]    [Pg.112]    [Pg.113]    [Pg.33]    [Pg.220]    [Pg.56]    [Pg.90]    [Pg.190]    [Pg.252]    [Pg.53]    [Pg.224]    [Pg.114]    [Pg.204]    [Pg.43]    [Pg.110]    [Pg.178]    [Pg.209]    [Pg.21]    [Pg.4]    [Pg.53]    [Pg.100]    [Pg.199]    [Pg.220]    [Pg.224]   
See also in sourсe #XX -- [ Pg.790 , Pg.792 , Pg.809 , Pg.812 ]




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