Methyl Hexyl Ketone

Place 80 g, of hydroxylamine sulphate (or 68-5 g. of the hydrochloride), 25 g. of hydrated sodium acetate, and 100 ml. of water in a 500 ml. flask fitted with a stirrer and a reflux water-condenser, and heat the stirred solution to 55-60°. Run in 35 g (42 nil,) of -hexyl methyl ketone, and continue the heating and vigorous stirring for ij hours. (The mixture can conveniently be set aside overnight after this stage.) Extract the oily oxime from the cold mixture twice with ether. Wash the united ethereal extract once with a small quantity of water, and dry it with sodium sulphate. Then distil off the ether from the filtered extract, preferably using a distillation flask of type shown in Fig. 41 (p. 65) and of ca, 50 ml, capacity, the extract being run in as fast as the ether distils, and then fractionally distil the oxime at water-pump pressure. Collect the liquid ketoxime, b.p. 110-111713 mm. Yield, 30-32 g. 

Hexyl methyl ketone, o36 Hexyl propyl ketone, d20 Hippuric acid, b70 Homocysteine, a200 Homopiperidine, h48 Homoveratric acid, d513 Homoveratrylamine, d517 Hydroacrylonitrile, hi 73 2-Hydrazinoethanol, hi 25... 

A022 CaHxeO hexyl methyl ketone 6vi CH3CO(CH2)5CHs EtOH at P0 KOH 1 - - - -/- 0-2 -... 

Hexyl methyl ketone, o34 Hexyl propyl ketone, dl6 Hippuric acid, b71 Histamine, i8 Homocysteine, a204 Homopiperidine, h51 Homoserines, al88, al89 Homoveratric acid, d447 Homoveratrylamine, d451... 

Cognate preparation. Hexyl methyl ketoxime. From hexyl methyl ketone (octan-2-one) (Expt 5.86) in 90 per cent yield b.p. 106-108 °C/12 mmHg. 

D.6) (D.6) 2-Octanone, octan-2-one, hexyl methyl ketone [111-13-7] FEMA 2802... 

N-Hexyl methacrylate. See Hexyl methacrylate Hexyl methyl ketone. See Methyl hexyl ketone Hexyl 2-methyl-2-propenoate. See Hexyl methacrylate... 

Synonyms Hexyl methyl ketone 2-Octanone Empirical CjHisO Formula CH,(CH2)5COCH,... 

D, dodecane DCIE, 1,2-dichlorethane DOS, di-n-octyl sebacate HMK, hexyl methyl ketone... 

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