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Glycopeptide complex Magnum 40 column separation

Figure 9a. Small-scale preparative separation of glycopeptide complex on Magnum 40 column (4.5 x 50 cm). Sample purified antibiotic (2 g). Column Whatman Partisil Prep 40 0DS-3 (37-60 jxm). Mobile phase 20 to 26% acetonitrile in 0.1 M KH2PO4PH 6.0. Flow 100 ml/min. Detection 210 nm. Figure 9a. Small-scale preparative separation of glycopeptide complex on Magnum 40 column (4.5 x 50 cm). Sample purified antibiotic (2 g). Column Whatman Partisil Prep 40 0DS-3 (37-60 jxm). Mobile phase 20 to 26% acetonitrile in 0.1 M KH2PO4PH 6.0. Flow 100 ml/min. Detection 210 nm.
Figure 9b. Recovery data for small-scale separation of glycopeptide complex on Magnum 40 column. Sample purified component I. Column Beckman Ultrasphere 0DS, 5 xm, 4.6 x 150 mm). Figure 9b. Recovery data for small-scale separation of glycopeptide complex on Magnum 40 column. Sample purified component I. Column Beckman Ultrasphere 0DS, 5 xm, 4.6 x 150 mm).

See also in sourсe #XX -- [ Pg.8 , Pg.79 ]




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