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Glyceryl Phenyl Ether

To 500 cc. of absolute alcohol (Note i) in a i-l. flask fitted with a reflux condenser is added gradually 46 g. (2 moles) of sodium in thin slices (Note 2) at such a rate that the mixture boils steadily. When all the sodium has been added, the mixture is heated on the steam bath until the few remaining pieces of sodium barely react. Pure commercial molten phenol is now added gradually through the condenser until all of the sodium has reacted, and then the remainder of 188 g. (2 moles) of phenol is added. This is followed by the addition of 221 g. (2 moles) of redistilled glycerol a-monochlorohydrin (Org. Syn. 2, 33) in small portions, the rather vigorous reaction being allowed to complete itself before each subsequent addition. [Pg.48]

Absolute alcohol is required in order that all the sodium chloride formed may be precipitated and that none may remain to contaminate the product. [Pg.49]

Vigorous mechanical stirring may be used to advantage in place of shaking by hand. [Pg.49]

The precipitate of sodium chloride obtained is very sludgy and filters poorly through fine-fibered papers. [Pg.49]

PEG-7 glyceryl cocoate PPG-10 cetyl ether Propylene glycol phenyl ether coupling agent, petrochemicals Oleyl alcohol... [Pg.5035]

Paper Chromatography.—Solvent systems have been developed for the separation of trichloromethyl- phenyl-, and pentafiuorophenyl-phosphonic and -phosphinic acids. Phosphoramidates and their hydrolysis products have been chromatographed, using triethylamine as a buffer. Silica gel on glass-fibre sheets may be used to separate inositol from its phosphate and to analyse phosphatide glyceryl ethers. ... [Pg.271]

Phenethyl salicylate Phenethyl tiglate Phenoxyacetaldehyde Phenoxyacetic acid Phenoxyethyl isobutyrate Phenoxyethyl propionate Phenylacetaldehyde Phenylacetaldehyde dimethyl acetal Phenylacetaldehyde glyceryl acetal Phenylacetaldehyde glyceryl cyclic acetals Phenylacetic acid Phenylacetonitrile o-Phenyl anisole 2-Phenylethyl acetate 2-Phenylethyl methyl ether... [Pg.5324]

Dimethyl 1,4-cyclohexanedicarboxylate polyester synthesis Phenyl acetate polyester, unsat. air curing Glyceryl-1-allyl ether... [Pg.5555]

See other pages where Glyceryl Phenyl Ether is mentioned: [Pg.48]    [Pg.49]    [Pg.135]    [Pg.575]    [Pg.89]    [Pg.138]    [Pg.89]    [Pg.138]    [Pg.48]    [Pg.49]    [Pg.135]    [Pg.575]    [Pg.89]    [Pg.138]    [Pg.89]    [Pg.138]    [Pg.233]    [Pg.1489]    [Pg.736]    [Pg.736]    [Pg.736]    [Pg.716]    [Pg.14]    [Pg.1883]    [Pg.355]    [Pg.29]    [Pg.202]    [Pg.5070]    [Pg.577]    [Pg.2534]   


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Ethers phenylic

Glyceryl

Phenyl Ether

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