Fuson

Bellamy, The Infra-Red Spectra of Complex Molecules, 1954 (Methuen). Randall, Fowler, Fuson and Dangl, Infrared Determination of Organic Structures, 1942 (Van Nostrand). 

See, for example, the following laboratory texts (a) Sorum, C. H. Lagowski, J. J. Introduction to Semimicro Qualitative Analysis, 5th ed. Prentice-Hall Englewood Cliffs, NJ, 1977. (b) Shriner, R. L. Fuson, R. C. Curtin, D. Y. The Systematic Identification of Organic Compounds, 5th ed. John Wiley and Sons New York, 1964. 

R. C. Fuson, Hdvanced Organic Chemistry, ]ohxi Wiley Sons, Inc., New York, 1950. 

Submitted by Lester Friedman and Edward Kosower. Checked by Reynold C. Fuson and Elliott N. Marvell. 

Ketone moschus (4-tcrt-butyl-2,6-dimethyl-3,5-dinitroacetophenone) [81-14-1] M 234.1, m 134-137 , 137-138 . Purified by recryst from MeOH. [Fuson et al. J Org Chem 12 587 1947.]... 

M, Randall, R. G. Fowler, N. Fuson, and J. R. Dangl, Infrared Determination of Organic Structures. Van Nostrand, New York, 1949. 

N-ethyl-3-chloropiperidine was prepared according to the method of Fuson and Zirkle described in Volume 70, J. Am. them. Soc., p 2760. 12.0 g (0.0B1 mol) of N-ethyl-3-chloropiperidine was mixed with 1B.6 g (0.0B1 mol) of benzilic acid and 80 cc of anhydrous isopropyl alcohol as a solvent. The mixture was refluxed for 72 hours. The solution was then filtered and concentrated at 30 mm of mercury. The concentrate was dissolved in water, acidified with hydrochloric acid and extracted with ether to remove the unreacted benzilic acid. 

Benzoin (Coll. Vol. 1, 88) From phenylglyoxal and benzene in the presence of aluminum chloride, in 90 per cent yield. Arnold and Fuson, J. Am. Chem. Soc. 58, 1295 (1936). 

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