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Fert-Butyldimethylsilyl chloride

Another analytical procedure for the extraction of degradation products of chemical munitions from water was developed by Sng and Ng. The technique is based on in situ derivatization by SPME. They investigated, for example, the derivatization of thiodiglycerol and ethyl-2-hydroxy ethyl sulfide. The derivatization reagent A-methyl-A-(tert-butyl-dimethylsilyl) trifiuoroacetamide with 1% fert-butyldimethylsilyl chloride, which forms hydrolytically stable ferf-butyldimethylsilyl derivatives, was used. Detection limits in the ppb range were realized with GC-MS in full scan mode. [Pg.355]

Scheme 9 Alkylation with sec-alkyl halides and fert-butyldimethylsilyl chloride... Scheme 9 Alkylation with sec-alkyl halides and fert-butyldimethylsilyl chloride...
See other pages where Fert-Butyldimethylsilyl chloride is mentioned: [Pg.60]    [Pg.2319]    [Pg.60]    [Pg.2319]    [Pg.619]    [Pg.131]    [Pg.472]    [Pg.225]    [Pg.260]    [Pg.485]    [Pg.33]    [Pg.36]    [Pg.521]    [Pg.382]    [Pg.212]    [Pg.280]   
See also in sourсe #XX -- [ Pg.7 ]



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