Dushman Reaction Investigated in Micro Reactors

3 Dushman Reaction Investigated in Micro Reactors Organic synthesis 91 [OS 91] Redox reaction of iodate and iodide 

This reaction is the reverse hydrolysis of iodine [22], In a further reaction, the product iodine reacts with iodide to give triodide. Both iodine and triodide absorb in the visible region, hence the reaction can be monitored optically. 

Processing in the micro reactor was analyzed by a CCD camera with a long working distance magnifying lens [22]. Visible spectrometry was applied for in-line sensing. The change in product concentration was determined at 450 nm. The light was collected via an optical fiber and sent to the spectrometer. 

5 Typical Results Flow rate/residence time 

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