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Double angle rotation probe

Fluorine-probe protocol has been applied to solid-state magic-angle spinning (SSMAS) 19F NMR analysis with the radiofrequency-driven dipolar recoupling (RFDR) method to measure the F-F distance in the microtubule-bound conformation of F2-10-Ac-docetaxel (see Figure 1.29a) [167], Moreover, five intramolecular distances of the key atoms in the microtubule-bound l9I72II/l3(Mabeled paclitaxel were determined by the rotational echo double resonance (REDOR) method (see Figure 1.29b and c) [168, 169],... [Pg.34]

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