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2,4 Dinitrophenylsulfur chloride

Practically the same method can be used for the preparation of o-nitro- -chlorophenylsulfur chloride (m.p. 95—970) the chlorination of the disulfide (m.p. 212-213°) in this case proceeds much more slowly. 2,4-Dinitrophenylsulfur chloride can be prepared by the chlorination of the corresponding disulfide in nitrobenzene suspension at 120-130°. As the chloride is of an explosive nature the solvent must be removed by distillation in vacuo at 130°. The crude material melts at 89-92°. After crystallization from carbon tetrachloride it melts at 94-95°. [Pg.46]

See other pages where 2,4 Dinitrophenylsulfur chloride is mentioned: [Pg.50]    [Pg.53]    [Pg.50]    [Pg.53]   
See also in sourсe #XX -- [ Pg.16 , Pg.46 ]

See also in sourсe #XX -- [ Pg.15 , Pg.46 ]

See also in sourсe #XX -- [ Pg.15 , Pg.46 ]

See also in sourсe #XX -- [ Pg.15 , Pg.46 ]



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