Cyperus conglomeratus

Normal-phase TLC has been employed for the separation of two new flavans in the extract of the undergorund tubers of Cyperus conglomeratus Rottb. (family Cyperaceae). The underground tubes were dried, ground and were extracted with with petroleum ether diethyl ether-methanol (1 1 1, v/v) for 24 h at ambient temperature. The extract was defatted with cold methanol. The components of the extract were preliminarily separated by traditional column chromatography followed by GC/MS and TLC. New flavans (5-hydroxy-7,3, 5 -trimethoxyflavan and 5,7-hydroxy-3, 5 -dimethoxyflavan) were separated on silica TLC layers using petroleum ether-diethyl ether (1 3, v/v) with the RF values of 0.50 and 0.37 for dimethoxy and trimethoxy derivatives, respectively [115]. 

Abdel-Mogib, M., Baisaf, S. A., and Ezmirly, S.T., Two novel flavans from Cyperus conglomeratus, Pharmazie, 55, 693, 2000. 

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