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Butyl Hypochlorite .Warning

Butyl hypochlorite, warning, 44, 26 N-chlorination of amines with, 41, 82 n-Butyl isocyanide, 41,14 /er/-Butyl isocyanide, 41,14 -Butylmagnesium bromide, 41, 61 reaction with rec-butyl crotonate, 41, 61... [Pg.56]

Butyl h3q)Ochlorite has been prepared by treatment of an alkaline solution of /-butyl alcohol with chlorine, - and a recent warning cautions against allowing the temperature to rise above 20° during this reaction. /-Butyl hypochlorite has been prepared in solution by shaking a solution of the alcohol in carbon tetrachloride, fluorotrichloromethane (Freon 11), and other solvents with aqueous hypochlorous acid. It has also been prepared by the action of chlorine on an aqueous /-butyl alcohol suspension of calcium carbonate, and by the action of chlorine monoxide on a carbon tetrachloride solution of the alcohol. ... [Pg.88]




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Butyl hypochlorite

Warnings

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