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Boron trichloride, purification

Reaction of H2(OEP) and diborane in THF and subsequent alkolysis gave (ROB)20 (OEP) (Scheme 3), while (HO)2B 2(TPP) was obtained after chromatographic purification of the unstable reaction product of H2(TPP) and boron trichloride (Scheme 4).24 Their structures have not been confirmed. They are slowly hydrolyzed in aqueous ethanol and rapidly in acid. [Pg.821]

Boron trichloride, BCI3. Mol. wt. 117.19, b.p. 13°. Supplier Matheson. Review. Purification through the nitrobenzene addition compound. ... [Pg.767]


See other pages where Boron trichloride, purification is mentioned: [Pg.404]    [Pg.121]    [Pg.123]    [Pg.147]    [Pg.371]    [Pg.371]    [Pg.53]    [Pg.404]    [Pg.75]    [Pg.1288]    [Pg.454]    [Pg.397]    [Pg.121]    [Pg.123]    [Pg.145]    [Pg.407]    [Pg.565]    [Pg.208]   
See also in sourсe #XX -- [ Pg.214 ]




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Boron trichloride

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