Bis diethylamino hydridoaluminum

The infrared spectrum of neat HA1[N(C2H5)2]2 exhibits Al—H stretching and deformation frequencies at 1822 and 692 cm 1, respectively. The compound can be distilled under high vacuum using a short-path distillation apparatus. It decomposes at 240° to give products of unknown composition.6 The compound can be stored indefinitely at room temperature in an oxygen- and water-free environment. 

Herbert O. House, Modern Synthetic Reactions, 2d ed., W. A. Benjamin, Inc., Menlo Park, Calif., 1972. 

Belgian Patent 654,406 (April 15, 1965) Chem. Abstr., 64, 9927g (1966). 

Marconi, A. Mazzei, F. Bonati, and M. deMalde, Gazz. Chim. Ital., 92, 1062 (1962). 

Shriver, The Manipulation of Air-Sensitive Compounds, McGraw-Hill Book Company, New York, 1969. 

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