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BENZOYL CHLORIDE, 4-PENTYL

Pentanol (0.2 mol) was added to 1.8 ml water dissolved in toluene (80 g) and hydrogen chloride gas (0.4 mol) introduced. The temperature was lowered to 0°C, 2-(chloromethyl)-benzoyl cyanide (0.09 mol) added dropwise, and the mixture stirred 2 hours at ambient temperature. Thereafter, the mixture was heated to 60 °C 8 hours then cooled. It was extracted once with 50 ml of 15% strength HCl, 3 times with 50 ml water, dried, concentrated, and isolated in 95% yield but containing 4.99% of the impurity, pentyl... [Pg.323]

See other pages where BENZOYL CHLORIDE, 4-PENTYL is mentioned: [Pg.5]    [Pg.79]    [Pg.98]    [Pg.8]    [Pg.13]    [Pg.159]    [Pg.5]    [Pg.79]    [Pg.98]    [Pg.8]    [Pg.13]    [Pg.581]   
See also in sourсe #XX -- [ Pg.7 , Pg.8 , Pg.61 ]

See also in sourсe #XX -- [ Pg.8 , Pg.61 ]

See also in sourсe #XX -- [ Pg.7 , Pg.8 , Pg.61 ]



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1- Pentyl

Benzoyl chloride

Benzoyl chloride, benzoylation

Pentylated

Pentylation

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