Benzoyl Azidodithiocarbonate

Benzoyl Azidodithiocarbonate A633-L Ben zoylazidomethane or m-Azidoaceto-phenone under Acetophenone. A47-R Benzozone or Acetyibenzoylperoxide A54-R Benzyl Abietate. See under Abietic Acid A3-R... 

Benzoyl Azidoditbiocarbonate, C6Hj CO-" SCSNs, mw 223.28, N 18.82% col monocl plates, mp 92-4°(dec) very sol in CHClj, moderately sol in eth, benz, CSa or CC14 and si sol in acet, EtOAc, ale or MeOH. It was prepd by the interaction of benzoyl chloride and Na azidodithiocarbonate, either in aq soln or in acet. The product was purified by crystn from chlf... 

QH, )jCH-SCSN raw 285.40, N 14.72% col ciysts, mp 67 very sol in acet, EtOAc, benz, CS, CHClj or CQ4, moderately sol in ale, MeOH or ech. It was prepd by the interaction of benzobydryl bromide and Na azidodithiocarbonate. After filtering to re move the pptd NaBr, the yel liq, separated by the addn of w, was dissolved in eth and benz which, after drying and cooling, separated in small col ciysts Benzoyl Azidoditbiocarbonate, QHs C0 sesNj, mw 223.28, N 18.82% col monocl plates, mp 92-4°(dec) very sol in CHCl, moderately sol in ech, benz, CS] or CCl and si sol in acet, EtOAc, ale or MeOH. It was prepd by the interaction of benzoyl chloride and Na azidodithiocarbonate, either in aq soln or in acet. The product was purified by crystn from chlf... 

Benzohydryl Azidodithiocarbonate A633-L l,2,3-Benzottiazino[3,4-a] periraidine. See under Aminophenylperimidines A246-L Benzoylacetylperoxide or Acetyl benzoyl-peroxide A54-R... 

---