Ammonium, tetrabutyl tetrachlorooxotechnetate

Tetrachlorooxotechnetate(V) results from action of cone. HC1 on perteeh-netate at ambient temperatures and is preferably isolated as the tetrabutyl-ammonium salt [19]. Tetrabromooxotechnetate(V) was similarly obtained with hydrobromic add at 0 °C [8]. The molecular structures of both compounds are reported in [20,21]. The analogous iodo complex, tetraiodooxotechnetate(V), was synthesized by ligand exchange of the chloro compound with sodium iodide in acetone [22]. However, it suffers from considerable decomposition during isolation. 

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See also in sourсe #XX -- [ , ]

See also in sourсe #XX -- [ , ]

See also in sourсe #XX -- [ , ]

See also in sourсe #XX -- [ , ]

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