The first experiment - what to do

Some typical experiments are detailed below, but first we must check the basics  

The above is only an illustration of likely scenarios. However, it is often usefirl to perform a wide-range thermal scan (— 100-300°C, or the melting point, if known) at two frequencies (1 and 10 Hz for example). This allows easy distinction between Tg and via the frequency dependence of data. Generally, the experimental methods are best considered with real data and such examples are given in Section 4.5. However, a brief description of experiment types is given below. 

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