Tetraethylammonium cZoso-l-Carba-dodecaboranate

Impurities in the BH3(SMe2) and solvent can sometimes result in a gummy yellow material at this stage. If this is the case, then an intermediate crystallization may be effected by dissolution in a minimum of hot ethanol and cooling to room temperature. [Pg.179]

B10H14 + KOH + 2H2O + PhCHO - [K][6-Ph-nido-6-CB9Hn] + B(OH)3 + 3H2 [K][6-Ph-nido-6-CB9Hii] + [NEt4]Cl [NEt4][6-Ph-mdo-6-CB9Hu] + KCl [Pg.180]

We thank the UK EPSRC and the UK DTI for support, and Professor Dwayne Heard for his good offices. [Pg.184]

in Boron Hydride Chemistry, E. L. Muetterties, ed., Academic Press, New York, 1973, [Pg.184]

Dolansky, and J. Duben, Collect. Czech. Chem. CommutL 46, 2345 (1981). [Pg.184]

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