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Silane-1,1-dithiolates

Reacting Me2SiCl2 with H2S at —78 °C gives the silane dithiol as an unstable oil which shows vs-h stretching at 2500 cm-1. The alkali metal derivatives of this dithiol result from the sulphide M2S (M = Li, Na, K) and react with RI (R = Me, Et) to give the bis... [Pg.1875]

The reduction of l,2-dithiole-3-thiones (7) by means of triethylsilane probably involves an addition of the silane to the thiocarbonyl group with subsequent opening of the ring and reaction with one further mole of triethylsilane123 (Eq. 4). [Pg.82]

See other pages where Silane-1,1-dithiolates is mentioned: [Pg.618]    [Pg.618]    [Pg.618]    [Pg.618]    [Pg.220]    [Pg.618]    [Pg.618]    [Pg.115]    [Pg.1872]    [Pg.151]    [Pg.106]    [Pg.618]    [Pg.618]    [Pg.4384]    [Pg.6172]    [Pg.78]    [Pg.1872]    [Pg.454]    [Pg.122]    [Pg.90]    [Pg.9]   
See also in sourсe #XX -- [ Pg.618 ]

See also in sourсe #XX -- [ Pg.618 ]



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