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Rotory Evaporator

The oily residue that separated was dissolved in CH2CI2, washed 3x with water, and dried over anhydrous MgSO. The solution was filtered and concentrated using a rotory evaporator. The residue was... [Pg.326]

Removal of the solvent on a rotory evaporator (water bath temperature 60°C) yields 2,3-epoxygeraniol as a slightly coloured oil (about 7.9 g, 87%). The product may be further purified by formation of its acetate followed by vacuum distillation (0.025 mmHg, 104-106°C) to yield 2,3-epoxygeranyl acetate as a colourless liquid containing only traces of its 6,7-isomer. ... [Pg.13]

See other pages where Rotory Evaporator is mentioned: [Pg.26]    [Pg.14]    [Pg.41]    [Pg.42]    [Pg.46]    [Pg.684]    [Pg.26]    [Pg.14]    [Pg.41]    [Pg.42]    [Pg.46]    [Pg.684]   
See also in sourсe #XX -- [ Pg.684 ]



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