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Rhodium-Catalyzed Synthesis of 2, 4, 5, 7-Tetraphenylisoindoline

2-(2-Methoxy-1-naphthyl)-6-phenyl-7,8-dihydro-5H-cyclopenta-[c]pyridine [Pg.482]

A thermostated reaction vessel is loaded with l-(l,6-Heptadiynyl)-2-methoxynaphthalene (497 mg, 2 mmol), benzonitrile (3, 412 pi, 4 mmol) and CpCo(COD) (5mol%) in THF (20 ml), under an argon atmosphere [15]. The mixture is stirred thoroughly and irradiated by two 460W lamps (/la420nm) for 24-72h. The [Pg.482]


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