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Proton-detected local field spectroscopy

A novel MAS NMR approach has been presented for the determination of motionally averaged heteronuclear dipolar couplings in unoriented materials. The technique is based on the proton-detected local field protocol and achieves dipolar recoupling by R-type RF irradiation. The experiment, which is called R-PDLF spectroscopy, is demonstrated on solid and liquid-crystalline systems. For mobile systems, it is shown that the R-PDLF scheme provides better dipolar resolution as compared to techniques combining conventional separated local field spectroscopy with R-type recoupling. [Pg.263]

See other pages where Proton-detected local field spectroscopy is mentioned: [Pg.85]    [Pg.524]    [Pg.636]    [Pg.86]    [Pg.91]    [Pg.498]    [Pg.65]    [Pg.193]    [Pg.2]    [Pg.111]    [Pg.200]    [Pg.172]    [Pg.329]    [Pg.124]    [Pg.193]    [Pg.171]    [Pg.311]    [Pg.572]    [Pg.212]    [Pg.551]    [Pg.455]   
See also in sourсe #XX -- [ Pg.85 , Pg.91 , Pg.92 ]



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Detection spectroscopy

Field detection

Local fields

Localized spectroscopy

Proton detection

Proton-detected local field

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