Powder Synthesis and Characterization

Si N powders were produced via laser-driven gas phase reactions. Details of the process have been reported elsewhere, and therefore are only 

Synthesized powders were subjected to the following battery or characterization methods X-ray and electron diffraction, He-pycnometry, single point BET gas absorption, TEM, XPS analysis based on a 101.3 eV silicon 2p binding energy for stoichiometric SigN powders neutron activation, and wet chemical analysis. The activity of SijN powders, both exposed and unexposed, was determined by measuring the surface area of powders annealed in nitrogen as a function of temperature. 

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Chang YS, Chang YH, Chen IG, Chen GJ, Chai YL (2002) Synthesis and characterization of zinc titanate nano-crystal powders by sol-gel technique. J Cryst Growth 243 319-326... 

Mehmet A. Gtilgtin, Oludele O. Popoola, Waltraud M. Kriven, Chemical synthesis and characterization of calcium aluminate powders , Journal of American Creamic Society 77[2], 531-539 (1994). 

Goellner, J. P, and Gates, B. G, Synthesis and characterization of site-isolated hexarhodium clusters on titania powder. J. Phys. Chem. B. 105, 3269 (2001). 

C.-C. Chuang, H.-l. Hsiang, J. S. Hwang, and T. S. Wang, Synthesis and Characterization of Al2O3-Ceo.5Zro.5O2 Powders Prepared by Chemical Coprecipitation Method, J. Alloys Compel, In Pressed, (2008). 

S. H. Chen and K. Kimura, Synthesis and characterization of carboxylate-modified gold nanoparticle powders dispersible in water, Langmuir, 15 (1999) 1075-1082. 

B. Sofiane, H. Didier, and L.P. Laurent, Synthesis and characterization of composite Hg-polyaniline powder material, Electrochim. Acta, 52, 62-67 (2006). 

SYNTHESIS AND CHARACTERIZATION OF Pd-POLYSILOXANE NANOCONJUGATES AS STABLE ISOLABLE POWDERS... 

Su J, Miao J-h, Xu L-h, Ji Y-q, Wang C-q (2012) Synthesis and characterization of nanociystalline Nd Ajoped gadolinium scandium aluminum garnet powders by a gel-combustion method. Mater Res Bull 47 1709-1712... 

Sohn S, Kwon Y, Kim Y, Kim D (2004) Synthesis and characterization of near-monodisperse yttria particles by homogeneous precipitation method. Powder Technol 142 136-153... 

Chen, W. Li, F. Yu, J. (2006). Combustion synthesis and characterization of nanociystalline Ce02-based powders via ethylene glycol-nitrate process. Material Letters, Vol. 60, No. 1, Ganuary 2006), pp. (57-62), ISSN 167-577X... 

Kim IS, Kumta PN. Sol-gel synthesis and characterization of nanostructured hydroxyapatite powder. Mater Sci Eng B-Solid 2004 111 232-6. 

Facchin G, Carturan G, Campostrini R, Lutterotti L, Armelao G, Marci L, et al. Sol-gel synthesis and characterization of Ti02 anatase powders containing nanometric platinum particles employed as catalysts. J Sol-Gel Sci Technol 2000 18 29-59. 

A. Celikkaya and M. Akinc, Synthesis and characterization of yttria powders by emulsion pre-... 

Benfer, S., Popp, U., Richter, H., Siewert, C., and Tomandl, G. (2001). Development and characterization of ceramic nanofiltration membranes. Sep. Purif. Technol 22-23 231-237. Vacassy, V., Guizard, C., Thoraval, V., and Cot, L. (1997). Synthesis and characterization of microporous zirconia powders application in nanofilters and nanofiltration characteristics. J Membr. Sci. 132 109-118. 

Synthesis and Characterization of Sintering Resistant Aerogel Complex Oxide Powders... 

Pratsinis SE (1998) Elame aerosol synthesis of ceramic powders. Prog Energy Combust Sci 24 197—219 Qi L, Ma J, Cheng H, Zhao Z (1998) Synthesis and characterization of mesostructured tin oxide with crystalline walls. Langmuir 14 2579-2581... 

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