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Oxidative Alkoxydifluorodesulfuration of Dithianylium Salts

Oxidative Alkoxydifluorodesulfuration of Dithianylium Salts A.7.1 Dithianylium Triflate 27 [Pg.287]

HS(CH2)3SH, CF3SO3H, toluene//-octane 1 1 reflux, azeotropic removal of HjO [Pg.287]

Scheme 2.72 Synthesis of liquid c stals by oxidative fluorodesulfuration of xanthogenates (aboi e) [162], and by the oxidative alkoxydifluorodesulfuration of dithianylium salts (beloiv) [163]. Scheme 2.72 Synthesis of liquid c stals by oxidative fluorodesulfuration of xanthogenates (aboi e) [162], and by the oxidative alkoxydifluorodesulfuration of dithianylium salts (beloiv) [163].


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Alkoxydifluorodesulfuration

Dithianylium salts

Oxidative alkoxydifluorodesulfuration

Oxidative dithianylium salts

Oxidizing salts

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