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Neutron reflection sample preparation

The crystal structure and hydrogen-bonding system in cellulose ip was elucidated by the combined use of synchrotron X-ray and neutron fiber diffraction." Oriented fibrous samples were prepared by aligning cellulose microcrystals from tunicin, reconstituted into oriented films. These samples diffracted both synchrotron X-rays and neutrons to a resolution better than 1 A, yielding more than 300 unique reflections and an unambiguous assignment of the monoclinic unit-cell dimensions (a = 7.784 A,... [Pg.45]


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See also in sourсe #XX -- [ Pg.59 ]




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