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Nectria episphaeria

Figure 1 shows the UV absorption spectrum of cephalochromin, a bis-napthopyrone metabolite of Nectria episphaeria see Fig. 6 for structure). This illustrates how distinctive (and thus diagnostic) a UV-absorbance profile can be for certain compound classes, particularly those containing a substantial number of conjugated carbon-carbon double bonds or aromatic rings. [Pg.173]

Figure 5 shows a gradient HPLC analysis of an extract of Nectria episphaeria fermentation broth. The two biologically active compounds of... [Pg.184]

Fig. 13. Preparative HPLC of cephalochromin from Nectria episphaeria. HPLC conditions Column Kromasil 7 Jin C8 25 x 5 cm. Mobile phase 50% v/v acetom-trile/50 mAf NH4H2PO4, 0.3.% v/v H3PO4. Flow rate 80 mL/min. Detection wavelength 210 ran. Sample load 190 mg (containing approx 50 mg dehydrocephalochromin/ cephalochromin) in 20 mL mobile phase. Fig. 13. Preparative HPLC of cephalochromin from Nectria episphaeria. HPLC conditions Column Kromasil 7 Jin C8 25 x 5 cm. Mobile phase 50% v/v acetom-trile/50 mAf NH4H2PO4, 0.3.% v/v H3PO4. Flow rate 80 mL/min. Detection wavelength 210 ran. Sample load 190 mg (containing approx 50 mg dehydrocephalochromin/ cephalochromin) in 20 mL mobile phase.

See also in sourсe #XX -- [ Pg.173 , Pg.184 , Pg.185 , Pg.186 , Pg.195 , Pg.196 ]




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