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N-HEXANE.218 Vol

Dodecylbenzyldiethylsulfonium Chloride. Into a 500 ml flask was added 76.6 g (0.200 moles) of- practical grade p-dodecylbenzyl chloride, 26.5 g (0.294 moles) diethyl sulfide (Eastman White label), 200 gof methanol and 2 g deionized water. Stirring was started and after 218.5 hrs the reaction was terminated by extracting it 3 times with 125 ml portions of a 50/50 (vol/vol) n-hexane/ether mixture. The aqueous fraction was separated and concentrated under vacuum to give 429 g of solution which was 19.8% active. The conversion was 85%. [Pg.292]

See other pages where N-HEXANE.218 Vol is mentioned: [Pg.396]    [Pg.404]    [Pg.390]    [Pg.398]    [Pg.385]    [Pg.392]    [Pg.389]    [Pg.396]    [Pg.389]    [Pg.396]    [Pg.385]    [Pg.392]    [Pg.344]    [Pg.351]    [Pg.396]    [Pg.404]    [Pg.390]    [Pg.398]    [Pg.385]    [Pg.392]    [Pg.389]    [Pg.396]    [Pg.389]    [Pg.396]    [Pg.385]    [Pg.392]    [Pg.344]    [Pg.351]   
See also in sourсe #XX -- [ Pg.2 ]



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N-Hexane

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