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Multiple microcoil probes

Figure 7.3.1.7 A 13C-decoupled HMQC spectrum of 54 mM chloroquine diphosphate in D2O acquired with an inverse detection microcoil probe. The 740-nl F0bs contained 40 nmol (13 jig) of chloroquine. The data, 32 transients per slice, 1024 x 128 (x2, hypercomplex) points, were acquired in 3.6h. The data were zero-filled to 256 points in the 13C dimension. A 40° shifted sinebell function was applied, followed by Gaussian multiplication prior to Fourier transformation... Figure 7.3.1.7 A 13C-decoupled HMQC spectrum of 54 mM chloroquine diphosphate in D2O acquired with an inverse detection microcoil probe. The 740-nl F0bs contained 40 nmol (13 jig) of chloroquine. The data, 32 transients per slice, 1024 x 128 (x2, hypercomplex) points, were acquired in 3.6h. The data were zero-filled to 256 points in the 13C dimension. A 40° shifted sinebell function was applied, followed by Gaussian multiplication prior to Fourier transformation...
R354 O. Goekay and K. Albert, From Single to Multiple Microcoil Flow Probe NMR and Related Capillary Techniques A Review , Anal. Bioanal. Chem., [online computer file], 2012, 402, 647. [Pg.46]

See other pages where Multiple microcoil probes is mentioned: [Pg.318]    [Pg.318]    [Pg.124]    [Pg.133]    [Pg.137]    [Pg.356]    [Pg.234]    [Pg.325]    [Pg.397]    [Pg.382]    [Pg.227]    [Pg.3]    [Pg.20]    [Pg.915]    [Pg.20]   
See also in sourсe #XX -- [ Pg.317 ]



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