Mixed Methylcyclohexenes

On occasion bromomethanesulfonyl bromide undergoes spontaneous, exothermic addition to olefins. While this problem was not encountered with 1-methylcyclohexene, it is desirable to mix the reagents at low temperature to avoid a possible vigorous spontaneous reaction and to maximize the yield of adduct. [Pg.195]

Figure 5.10 Rotational diffusion times of mixed (O) methylcyclohexene and ( ) chloronaphthalene, each as a function of its own mole fraction, based on results of Gisser and Ediger(41). This system is a binary mixture, so that if one solvent has X = 1 the other solvent has jc 0.

$Figure 5.10 Rotational diffusion times of mixed (O) methylcyclohexene and ( ) chloronaphthalene, each as a function of its own mole fraction, based on results of Gisser and Ediger(41). This system is a binary mixture, so that if one solvent has X = 1 the other solvent has jc 0.$

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