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Methyl santolinate

The efficient addition of allylic bromides to carbonyl compounds in a heated zinc column has been used to synthesize ( )-artemisia alcohol (81 R = H, X = CH2) in 91% yield.Artemisia ketone was synthesized efficiently from 3-methyl-l-trimethylsilylbut-2-ene and 3-methylbut-2-enoyl chloride in the presence of AlCls. Racemic methyl santolinate (82) was synthesized (along with the C-3 epimer ratio 8 1) via Claisen rearrangement, according to Scheme 2 (cf. Vol. 6, p. 7). ... [Pg.21]

See other pages where Methyl santolinate is mentioned: [Pg.212]    [Pg.51]    [Pg.165]    [Pg.212]    [Pg.51]    [Pg.165]   
See also in sourсe #XX -- [ Pg.3 ]



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