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Melt crystallization Kureha double screw purifier

Kureha Double-Screw Purifier [Fig. 16.16). This unit employs a double screw with intermeshing blades that express the liquid from the crystal mass as it is conveyed upward. The melt is formed at the top, washes the rising crystals countercurrently, and leaves as residue at the bottom. A commercial unit has an effective height of 2.6 m and a cross section of 0.31 m2. When recovering 99.97% p-dichlorbenzene from an 87% feed, the capacity is 7000 metric tons/yr. The feed stock comes from a tank crystallizer and filter. Data on other eutectic systems are shown, and also on separation of naphthalene and thiophene that form a solid solution a purity of 99.87% naphthalene is obtained in this equipment. [Pg.545]


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