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Magic angle spinning, single crystals

A. N. Klymachyov and N. S. Dalai, Magic angle spinning NMR on single crystals as a new aid in characterizing phase transitions application to squaric acid. Z. Phys. B, 1997,104, 651-656. [Pg.30]

It is also possible to measure the isotropic equivalent chemical shifts experimentally using magic angle spinning (MAS) on powder specimens. These experiments are much simpler than the single crystal measurements and require... [Pg.69]

The cross-polarization magic-angle-spinning NMR spectra of three structures (51-53) have shown the keto-hydroxy tautomerism in compound 51 but not in 52 and 53. This was confirmed by a single-crystal X-ray diffraction study of compound 51. The results revealed that the distinct molecules in the unit cell are linked by intermolecular hydrogen bonds. ... [Pg.729]

N.S. Dalai, K.L. Pierce, J. Palomar, R. Fu, Single-crystal magic-angle spinning O NMR and theoretical studies of the antiferroelectric phase transition in squaric acid,... [Pg.219]


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See also in sourсe #XX -- [ Pg.29 ]




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Magic angle spinning

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