Magic angle sample spinning

Cross Polarization-Magic Angle Sample Spinning NMR Studies... 

Moller, M. Cross Polarization — Magic Angle Sample Spinning NMR Studies. With Respect to the Rotational Isomeric States of Saturated Chain Molecules. Vol. 66, pp. 59-80. 

Stoll ME, Majors TJ, Elimination of magnetic-susceptibility broadening in NMR using magic-angle sample spinning to measure chemical shifts in niobium hydride (NbHx), J. Phys. Rev. B, 24 2859-2862, 1981. 

Garroway AN, Magic-angle sample spinning of liquids, J. Magn. Reson., 49 168-171, 1982. 

Mass WE, Laukien FH, Cory DG, Gradient, High resolution, magic angle sample spinning NMR, J. Am. Chem. Soc., 118 13085-13086, 1996. 

Silicon NMR measurements were made at 39.5 MHz on a Jeol FX200WB spectrometer using the combined techniques of magic-angle sample spinning and proton dipolar decoupling. All samples were examined in the fully hydrated state. Chemical shifts were referenced to sodium 4,4-dimethyl-4 silapentane sulfonate taken to... 

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