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Lysergic acid dimethylamide

Yield about 0.3 g. The sample thus obtained contains one molecule of benzene of crystallization which can he separated by heating the amide at 100° C. in high vacuo. The analysis values obtained correspond to the formula C18H210N3. The rac. lysergic acid dimethylamide is easily soluble in ethanol and acetone, rather dif cultly soluble in benzene and practically insoluble in water. It gives the blue Keller s colour reaction. Source Sandoz 1938... [Pg.55]

Examples The sample (rac. lysergic acid dimethylamide) thus obtained contains one molecule of benzene of crystallization which can be separated by heating the amide at 100° C. in high vacuo. Sandoz 1936... [Pg.80]

The conformation of the D-ring in the dimethylamides of lysergic acid and of isolysergic acid has been studied by H NMR spectroscopy. The lysergic acid derivative exists in the conformation [345] with the halfchair D-ring and the pseudo-equatorial amide function. This conformation is supported by allylic coupling between the 5- and 9-protons of... [Pg.112]

See other pages where Lysergic acid dimethylamide is mentioned: [Pg.365]    [Pg.112]    [Pg.159]    [Pg.173]    [Pg.46]    [Pg.54]    [Pg.22]    [Pg.251]    [Pg.253]    [Pg.365]    [Pg.112]    [Pg.159]    [Pg.173]    [Pg.46]    [Pg.54]    [Pg.22]    [Pg.251]    [Pg.253]    [Pg.280]   
See also in sourсe #XX -- [ Pg.173 , Pg.175 ]



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Dimethylamide

Racemic Lysergic Acid Dimethylamide

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