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Lithium aluminate peroxide

The synthesis of lithium aluminates for tritium production requires formation of nanostructured phases. These can be made by solid-state reaction, by appropriate mixing of oxide powders [84] or by sol-gel methods [80, 85-87], One technique is the peroxide route where y-Al203 and LiC03 are dissolved in a peroxide (H202) solution. Evaporation of water and calcining the solid residue results in nanophase LiA102. [Pg.60]

Caution. The reaction should be carried out in a well-ventilated hood and away from flames, since BMS, 1,3-butadiene, organoborane by-products, and methyl sulfide are flammable, odoriferous, and possibly toxic substances. BMS and the initial hydroboration product are sensitive to air and moisture. The inert atmosphere technique8 is therefore recommended. Peroxide-free tetrahydro-furan (THF) should be distilled from a small quantity of lithium tetrahydro-aluminate according to the procedures in Reference 8. BMS is a very concentrat-... [Pg.240]

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See also in sourсe #XX -- [ Pg.131 ]



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ALUMINIC

Alumin

Alumination

Aluminization

Lithium peroxide

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