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Lithiation Experimental Procedure

The reaction of lithiated S,S-acetals with aldehydes and ketones is a well-established reaction and needs no exemplification by an experimental procedure. The reactions with most of the aldehydes and ketones are extremely rapid, even at temperatures in the region of — 80 °C. A number of examples have been mentioned in the reviews of Seebach [1,2]. [Pg.66]

Modification of the experimental procedure used for the previous ortho lithiation strategies was necessary for the preparation of trifluoromethyl- and trifluoro-mefhoxy-substituted benzenesulfonyl chlorides. When 3-trifluoromethylanisole (24, PG = Me, Scheme 6) was subjected to conditions identical to those in... [Pg.92]

See other pages where Lithiation Experimental Procedure is mentioned: [Pg.1122]    [Pg.159]    [Pg.161]    [Pg.743]    [Pg.743]    [Pg.156]    [Pg.95]    [Pg.50]    [Pg.171]    [Pg.69]    [Pg.202]    [Pg.55]   
See also in sourсe #XX -- [ Pg.161 ]



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