Isco CombiFlash

General Experimental Procedures MPLC fractionation was performed using an Isco CombiFlash, and HPLC isolation was performed using Shimadzu pumps and detector and YMC-Pack ODS-AQ C18 column. 

Isco, Inc. The CombiFlash Sg 100c System is suitable for purifying 10 to 35 g of material. It provides time- or peak-based fraction collection with on-line UV detection, and a linear and/or step gradient with two solvents at a flow rate of 10 to 100 mL/min. 

Figure 1.6 (cent.) (B) CombiFlash Companion (reprinted with permission from Teledyne-ISCO). 

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