H-transfer reduction Investigated in Micro Reactors

3 H-transfer reduction Investigated in Micro Reactors Organic synthesis 63 [OS 63] H-transfer reduction of dimethyl itaconate [Pg.509]

This H-transfer reduction with sodium formate and employing catalysis by a water-soluble rhodium-phosphine catalyst yields dimethyl methylsuccinate [117]. [Pg.509]

Conversion/selectivity/yield - benchmarking to batch processing/kinetics [Pg.509]

Correction for liquid/liquid mass transfer resistance [Pg.509]

Main axis experimental conversions ( ) intrinsic kinetic model (solid line) kinetic model + mass transfer kinetics (dashed line). Secondary axis variation of computed k,o with flow rate. [Pg.509]