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Ge-NOESY-TOCSY

Fig. 18. The pulse sequence of a ID ge-NOESY-TOCSY experiment, tnoe is the NOE mixing time, 5 are optional delays which can be used for z-filtration [81] or for suppression of ROE effects in macromolecules (2 x (5 + Tgrad) = 0.5 x mixing time). DIPSI-2 [78] sequence was used for isotropic mixing. Phases were cycled as follows 0i = 2x, 2(—x) (j)2 = X, —x Ip = X, 2 —x), X. Rectangular PFGs, G = 6 Gauss/cm and Gi = 7 Gauss/cm, were applied along the axis for Xpad = 1 ms. Fig. 18. The pulse sequence of a ID ge-NOESY-TOCSY experiment, tnoe is the NOE mixing time, 5 are optional delays which can be used for z-filtration [81] or for suppression of ROE effects in macromolecules (2 x (5 + Tgrad) = 0.5 x mixing time). DIPSI-2 [78] sequence was used for isotropic mixing. Phases were cycled as follows 0i = 2x, 2(—x) (j)2 = X, —x Ip = X, 2 —x), X. Rectangular PFGs, G = 6 Gauss/cm and Gi = 7 Gauss/cm, were applied along the axis for Xpad = 1 ms.
The ID ge-NOESY-TOCSY experiment is illustrated using a EPS O-polysaccharide (7) isolated from Proteus mirabilis serotype 0 57 [79]. The... [Pg.84]

See other pages where Ge-NOESY-TOCSY is mentioned: [Pg.58]    [Pg.84]    [Pg.84]    [Pg.85]    [Pg.86]    [Pg.86]    [Pg.58]    [Pg.84]    [Pg.84]    [Pg.85]    [Pg.86]    [Pg.86]    [Pg.85]   
See also in sourсe #XX -- [ Pg.84 ]



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