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Gallium trichloride synthesis

A superior method involves the reaction of gallium trichloride with excess neat trimethylaluminum.4,5 The trimethylgallium is separated from the reaction mixture by distillation and purified further by distillation from sodium fluoride in order to remove any chlorodimethylaluminum. This synthesis produces a high yield of triiBthylgallium (ca. 63 %) in about 6 hours and may be run on any convenient scale. [Pg.203]

C9Hi6Cl3GaN02 2,2,6,6-Tetramethyl-4-piperidone 1-oxide gallium trichloride Nr.lO,X=GaCl3 Chemical synthesis from stable components/ Benzene EPR/ 300 N 1.81 (7) Ga 3.07 (5) Ga 3.89 (7) 69Abal... [Pg.320]

See other pages where Gallium trichloride synthesis is mentioned: [Pg.223]    [Pg.310]    [Pg.60]    [Pg.179]    [Pg.22]    [Pg.6]    [Pg.272]    [Pg.19]   


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Gallium trichloride

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