2-formylphenyl phenylthio

Formylphcnyl tellurium bromide and benzenethiol in refluxing pyridine produced 2-formylphenyl phenylthio tellurium2. 

Formylphenyl Phenylthio Tellurium2 2.5 g (8.0 mmol) of 2-formylphenyl tellurium bromide are dissolved in 25 ml of pyridine, 0.88 g (8.0 mmol) of benzenethiol are added, and the mixture is heated under reflux for 2 h. The resultant mixture is poured into aqueous hydrochloric acid/ice and extracted with chloroform. The organic phase is separated, dned, filtered, and chloroform is distilled from the filtrate. The residue is recrystallized from hexane/benzene yield 1.4 g (50%) m.p. 73°. 

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See also in sourсe #XX -- [ ]

See also in sourсe #XX -- [ ]

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