Fluorinations with Pyridinium Polyhydrogen Fluoride Reagent 1-FluoroADAMANTANE

FLUORINATIONS WITH PYRIDINIUM POLYHYDROGEN FLUORIDE REAGENT 1-FLUOROADAMANTANE [Pg.75]

Submitted by George A Olah and Michael Waikins1 Checked by Paul G Williard and G Buchi [Pg.75]

The recommended procedure for an HF burn is to flood with water, pack with ice, and get medical attention as quickly as possible. Local medical personnel should be alerted and prepared when work with HF is planned. Directions for proper medical treatment are given in reference 2. [Pg.76]

The submitters used A.C.S. certified reagent-grade pyridine from Fisher Scientific Company which was distilled from potassium hydroxide prior to use. [Pg.77]

The submitters obtained anhydrous HF from Harshaw Chemical Company, and the checkers purchased this reagent from Matheson Gas Products. [Pg.77]

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